Gave B99 the freezer test!

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The biodiesel I've been buying comes from Propel Fuels, which I think is buying it from Seattle Biodiesel and selling it Propel who markets it with SeaPort Petroleum, is that confusing enough? It'll be at least 8 month before my new garage is built and I get the biodiesel still setup, so I'll be using this pump bio through the winter. From what the people at SeaPort tell me, this is made from virgin canola oil, they used one other oil is canola was in short supply but I can't remember what they told me.


I pumped one quart (shy) of B99 into a mason jar and placed it into my refrigerator. I used a thermometer for HVAC vent measurements to determine my refrigerator maintains about 30-31*F. After 24 hours in the refer the B99 stayed very liquid, although somewhat cloudy throughout it retained it's yellow color. The bottom had a layer of wax fallout, I estimate the amount of wax to be about 20% of the total volume. Although this is certainly approaching the temperature limit of this fuel I can see no reason not to run this fuel down to freezing temperatures, which I see very seldom as the temperature staying about 40*F most of the winter.
[img=http://thumb4.webshots.com/t/53/453/5/22/33/2841522330096396344chlmcY_th.jpg]

I placed the sample back into the refer for about 2 hours to stabilize the temperature. After the temperature stabilized I added a small amount of Stanadyne Performance Formula fuel additive which is supposed to lower the pour point by 40*F from the fuel's original pour point. As my truck as a heated fuel filter/water separator the Cold Filter Plugging Point is not a concern, only the pour point. As long as the fuel pump can pull the fuel out of the tank my truck will run just fine. As long as I can get the truck running, the return fuel supply will warm the tank enough to allow proper operation.
[img=http://thumb4.webshots.com/t/28/28/8/99/7/2682899070096396344xUzBeh_th.jpg]
[img=http://thumb4.webshots.com/t/53/453/0/60/49/2949060490096396344OHURXF_th.jpg]


After the Stanadyne was added I again placed the sample in the refer to stabilize the temperature. After this period very little noticeable affect was observed. I then shook the sample to try and mix the Stanadyne with the B99. Some affect was observed, however not significant. What agitating the sample achieved was the size of the wax crystals were reduced and suspended more evenly.
[img=http://thumb4.webshots.com/t/57/757/8/22/14/2928822140096396344mqYzFi_th.jpg]


Directly after the shake test I warmed the sample to around 45*F to recombine approximately 98% of the wax back into the liquid fuel. When I was doing this I again agitated the sample. This should simulate the addition of the fuel additive to a tank of fuel and immediately operating the vehicle. This was most effective and by the time the sample was placed back into the refer no visible wax remained in the sample. The sample was placed back into the refer and the temperature once again stabilized.

The following pictures are after the last refrigerator run. The sample did could up some, however no wax settled out of the solution and laid on the bottom of the jar. I don't have a precise thermometer that will register below 25*F. I have order a low temperature thermometer so that I can see at what point the B99 with Stanadyne added will reach the pour point. I think that for my climate I can run pump B99 year round with little to no problem. For the colder parts of the winter pump B99 with some pour point depressant will work fine. If I'm going to be in mountain conditions longer than a day of skiing I will probably mix some dino diesel with the biodiesel which should virtually eliminate any problems I might have.
 
We do have a few nights here that may hit the teens. Very rare to have single digits. I am going to run B75 this winter. It will be my own home brew and 25% #1 diesel.

Thanks for the excellent write up. I was about to do something similar but you saved me a lot of work.

cheers.gif
 
I'm going to run B99 all winter I think. As long as I'm close to home it will be fine, and I don't drive the truck much unless I'm on vacation. If I'm going into colder weather, which is really just across the valley, I'll probably do as you suggest and run 25% #2 or #1. Since I don’t need to drive this everyday I’m going to push the temp limit and see in practice just how cold of ambient I can run in without major problems.
 
I Do not think that the BIO has any wax like a normal diesel. Most likely is unreacted fatty acid/ester called Unsaponifiables or Heavier higher carbon chain fats that have lower solubility.

Common in all animal/vegtable oils. Normal wax PPD do not work on this stuff do not work with fuels so do not know what will.

Guess you could "cold" filter to get out "stuff".
bruce
 
Thanks for the information bruce. Lubrizol has an additive that is biodiesel specific, but I'm not real sure on any details. I also see that PowerService has a biodiesel additive, however I found out that it is for a B20 blend, so they are really just addressing the dino diesel I would guess, which fits with your statements.

I did see a definite improvement with the addition of the Stanadyne. I haven't figure out what my actually treatment rate was, however I estimate it to be around 3 times what Stanadyne recommends for dino diesel. This is probably not cost effective for a reduction of CFPP of about 10*F.

The Lubrizol additive does not say it's for fuel, just for vegetable based oils. Elsewhere on their site they do mention additives for biodiesel specifically. I'd be curious to hear your opinion on the options and the Lubrizol additives bruce.
 
I'll look it up on the password site and see whats up if they have a PPD for Bio maybe I can send you a quart to play with.
bruce
 
I might order some of that as well. I left the sample above with the Stanadyne in the refrigerator for over a month now, and it still shows an improvement over the untreated pump bio. I also ran another test quart since they should have had to refill the bulk tank at least once.

I have some Soy Shield Winterized to try as well. Working 12-15 hour days right now so updates will be a little slow, but I'm still working on it.
 
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