I have had an issue with my Landrover service. I believed they did not change the oil, but I was charged for it. The oil should be a green colour, but after the service the oil was grey, so I sampled it and had it tested.
Here are the results, Oil sample taken 3 days after oil change.
1) Oil supposedly used in service:
PHYSICAL PROPERTIES
Viscosity @ 40°C cSt 54.9
Water Content %wt 0.0
PQ Index 13
SPECTROCHEMICAL ANALYSIS
Iron ppm 1
Chromium ppm 0
Aluminium ppm 3
Molybdenum ppm 108
Copper ppm 0
Lead ppm 0
Tin ppm 0
Nickel ppm 0
Silicon ppm 7
Sodium ppm 2
Boron ppm 72
Vanadium ppm 0
Calcium ppm 3151
Phosphorus ppm 746
Zinc ppm 818
Magnesium ppm 13
Barium ppm 1
2) Oil sample taken from engine:
PHYSICAL PROPERTIES
Viscosity @ 40°C cSt 55.3
Water Content %wt 0.0
PQ Index 10
SPECTROCHEMICAL ANALYSIS
Iron ppm 7
Chromium ppm 0
Aluminium ppm 5
Molybdenum ppm 107
Copper ppm 1
Lead ppm 0
Tin ppm 0
Nickel ppm 19
Silicon ppm 2
Sodium ppm 66
Boron ppm 0
Vanadium ppm 3026
Calcium ppm 763
Phosphorus ppm 860
Zinc ppm 92
Magnesium ppm 0
Barium ppm 1
Here are the results, Oil sample taken 3 days after oil change.
1) Oil supposedly used in service:
PHYSICAL PROPERTIES
Viscosity @ 40°C cSt 54.9
Water Content %wt 0.0
PQ Index 13
SPECTROCHEMICAL ANALYSIS
Iron ppm 1
Chromium ppm 0
Aluminium ppm 3
Molybdenum ppm 108
Copper ppm 0
Lead ppm 0
Tin ppm 0
Nickel ppm 0
Silicon ppm 7
Sodium ppm 2
Boron ppm 72
Vanadium ppm 0
Calcium ppm 3151
Phosphorus ppm 746
Zinc ppm 818
Magnesium ppm 13
Barium ppm 1
2) Oil sample taken from engine:
PHYSICAL PROPERTIES
Viscosity @ 40°C cSt 55.3
Water Content %wt 0.0
PQ Index 10
SPECTROCHEMICAL ANALYSIS
Iron ppm 7
Chromium ppm 0
Aluminium ppm 5
Molybdenum ppm 107
Copper ppm 1
Lead ppm 0
Tin ppm 0
Nickel ppm 19
Silicon ppm 2
Sodium ppm 66
Boron ppm 0
Vanadium ppm 3026
Calcium ppm 763
Phosphorus ppm 860
Zinc ppm 92
Magnesium ppm 0
Barium ppm 1