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#1581270 - 08/28/09 12:56 PM
3 diff. labs with samples taken frm the same bott
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Registered: 06/04/05
Posts: 1932
Loc: Vinegar Hill
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The chronology: I sent in a virgin sample to Blackstone for the generally highly regarded Petro Canada Supreme Synthetic (in this case its 0W30 entry). Looking at the numbers I was surprised by the calcium, phosphorus and zinc...all seemed low. Blackstone was kind enough to retest...the new numbers were similar. I contacted Petro Canada and they requested I submit a sample to them. He did tell me, prior to testing my sample, that he expected, based upon batch analysis that Calcium would be around 2230, Phosphorus 780 and Zinc 870. I have summarized the information below. (I have a full analysis for only Blackstone and Wearcheck) All samples were taken from the *same* bottle of new unopened oil.
Initial Blackstone Retest of same sample (Blackstone) In House Petro Canada Lab Wearcheck Canada
Calcium 1214 1196 2250 2015
Phosphorus 422 430 780 694
Zinc 572 554 940 814
Edited by 21Rouge (08/28/09 12:56 PM)
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#1581272 - 08/28/09 12:58 PM
Re: 3 diff. labs with samples taken frm the same bott
[Re: 21Rouge]
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Registered: 03/17/08
Posts: 4203
Loc: Michigan
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Hmmm. very interesting.
Edited by ZZman (08/28/09 12:58 PM)
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2002 Buick Regal GS (3.8 Supercharged) PP, Pure 1 filter 2008 Sebring Hardtop convertible (2.7) PP, MC filter.
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#1581288 - 08/28/09 01:21 PM
Re: 3 diff. labs with samples taken frm the same bott
[Re: ZZman]
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Registered: 11/20/06
Posts: 6631
Loc: MA, Mittelfranken.de
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Downright disturbing is what i call it. People buy oil,switch brands,weights etc based on the numbers coming out of these labs.
I never got into doing UOA because i question the value if a UOA on a single run of a specific brand then doing another on the latest craze trying to compare the two. Long term trends with the same product i would think may provide better results.
The way this looks it appears that some of these labs may be pulling numbers either from manufacturers spec sheets or out of their behind.
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ASE L1, Master. Deutsch Meisterbrief
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#1581291 - 08/28/09 01:26 PM
Re: 3 diff. labs with samples taken frm the same bott
[Re: Trav]
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Registered: 04/19/04
Posts: 4443
Loc: New York
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This tells me that my money is better spent changing my oil than analyzing it.
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#1581297 - 08/28/09 01:32 PM
Re: 3 diff. labs with samples taken frm the same bott
[Re: pbm]
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Registered: 09/19/08
Posts: 1378
Loc: Pennsylvania
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Amen. So when you look at these numbers from UOA, remeber that the standard deviations are apparently HUGE when looking at these numbers. It tells me that these numbers are virtually worthless.
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2003 Saturn L 300 M1 5W-30, Saturn Filter 2007 Frontier V-6 M1 5W-30 Pure One 14610
"Always gallop towards the guns; always walk away."
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#1581300 - 08/28/09 01:39 PM
Re: 3 diff. labs with samples taken frm the same b
[Re: Trav]
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Registered: 06/04/05
Posts: 1932
Loc: Vinegar Hill
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The way this looks it appears that some of these labs may be pulling numbers either from manufacturers spec sheets
FWIW I purposely did not tell Wearcheck the brand or viscosity of oil.
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#1581302 - 08/28/09 01:47 PM
Re: 3 diff. labs with samples taken frm the same b
[Re: Trav]
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Registered: 06/04/05
Posts: 1932
Loc: Vinegar Hill
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Long term trends with the same product i would think may provide better results.
+1, and now with the caveat that one uses the same lab! 
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#1581303 - 08/28/09 01:50 PM
Re: 3 diff. labs with samples taken frm the same b
[Re: 21Rouge]
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Registered: 01/29/09
Posts: 2671
Loc: NJ
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I wonder if additive fallout(some falling to the bottom) would cause numbers like that. I myself am no chemist and not sure if calcium itself can fall out of suspension in oil.
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2011 Malibu LS 2.4l Ecotec 5w20 Motorcraft Synthetic Blend 2011 Subaru Impreza 2.5i +Dealer Serviced
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#1581305 - 08/28/09 01:52 PM
Re: 3 diff. labs with samples taken frm the same b
[Re: Anies]
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Registered: 06/04/05
Posts: 1932
Loc: Vinegar Hill
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I wonder if additive fallout(some falling to the bottom) would cause numbers like that.
I promise I shook the bottle each time I drew a sample.
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#1581306 - 08/28/09 01:53 PM
Re: 3 diff. labs with samples taken frm the same b
[Re: 21Rouge]
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Registered: 02/07/08
Posts: 3825
Loc: Texas
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Now you know why I ain't doin' no UOAS.
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#1581307 - 08/28/09 01:54 PM
Re: 3 diff. labs with samples taken frm the same b
[Re: 21Rouge]
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Registered: 11/20/06
Posts: 6631
Loc: MA, Mittelfranken.de
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and now with the caveat that one uses the same lab! It would sure seem that way. Did you inform Petro what the sample was beforehand? The numbers seem real close to what he told you they would be, Do you get the feeling they just tweaked the numbers and actually tested nothing?
Edited by Trav (08/28/09 01:55 PM)
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ASE L1, Master. Deutsch Meisterbrief
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#1581314 - 08/28/09 01:58 PM
Re: 3 diff. labs with samples taken frm the same b
[Re: Trav]
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Registered: 09/08/05
Posts: 13243
Loc: Canada
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Wearcheck's numbers look spot-on. I'd believe them the most.
B/S is a a good lab, but when they shouldn't have stood by their numbers - they should have known something was off with their numbers, and investigated thoroughly.
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2003 Mazda Tribute LX V-6, 144K miles. M1 AFE 0W-20 and M1-210.
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#1581320 - 08/28/09 02:00 PM
Re: 3 diff. labs with samples taken frm the same b
[Re: Trav]
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Registered: 06/04/05
Posts: 1932
Loc: Vinegar Hill
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Did you inform Petro what the sample was beforehand? The numbers seem real close to what he told you they would be, Do you get the feeling they just tweaked the numbers and actually tested nothing?
For sure I told them as I only made contact with them because the Blackstone numbers didnt seem right...two tests in a row! So the company knew I was sending in another sample of their 0W30 from the same bottle. Of course I have no idea what was actually done with my sample but given my correspondence with their rep. I take it at face value that it was tested.
Edited by 21Rouge (08/28/09 02:10 PM)
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#1581354 - 08/28/09 02:40 PM
Re: 3 diff. labs with samples taken frm the same b
[Re: 21Rouge]
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Registered: 05/25/05
Posts: 3999
Loc: Calgary Canada
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The closeness of wearcheck to petrocan would make me suspect blackstone got the test/sample mixed up on first instance and fudged the numbers the second time. Just guessing though.
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Jim A 07.5 GMC Sierra 2500HD LMM Rotella 15w-40 09 Odyssey EX-L CT 5w-20 66 Bronco QS 10w-30 08 BMW K1200S Rt 15w-40 08 Pitster Pro X4 Rt 15w-40
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#1581357 - 08/28/09 02:42 PM
Re: 3 diff. labs with samples taken frm the same b
[Re: addyguy]
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Registered: 11/18/05
Posts: 7084
Loc: Burlington, Ontario, Canada
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Wearcheck's numbers look spot-on. I'd believe them the most.
B/S is a a good lab, but when they shouldn't have stood by their numbers - they should have known something was off with their numbers, and investigated thoroughly. +1 21Rouge, do you have the other VOA figures from Wearcheck including TBN?
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'74 Lotus Europa - 5W-50,VSOT '86 Porsche 928S - TGMO 0W-20/M1 0W-40 blend '96 BMW 328i - Idemitsu 0W-20/M1 0W-40 " '94 Caterham 7 - Sustina 0W-20
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